Showing posts with label soapmaking. Show all posts
Showing posts with label soapmaking. Show all posts

Sunday, November 21, 2010

Soap Making 2

I made soap today. I have an abundance of pork fat from the pig we butchered so instead of using just bison fat like I did my first time, I used pork lard too. I spent most of the time calculating the proportion of lye to fat. I had a reference that gave me the saponification values (SAP) for beef and pork fat. That is the amount of Potassium Hydroxide (KOH) in milligrams it takes to make soap out of one gram of fat. Beef tallow = 197 and Pork lard = 194.6.

I used a half pound of each and averaged the SAP value to 195.8. For one pound of fat I needed .1958 lbs. of lye. But since I used Sodium Hydroxide (NaOH), I had to multiply by the fraction 40/56.1 to get a proper conversion. Finally, to make the soap milder and less caustic to naturally acidic human skin I discounted the lye by another 15.5% to come up with a final number of .1179lbs. or 53.47 grams.

While this seems a bit complicated, it's pretty cool. Once you know the SAP values of various fats and oils you can concoct you own mixtures. This time I tried a relatively simple 50% bison/50% lard mixture, but in the future I could throw in olive oil or another type of oil. Each fat and oil has different properties that can affect the hardness, amount of lather and other characteristics of the finished product.

In this picture I weighed half a pound of beef tallow.



I mixed the beef tallow and pork lard together in a pan over low heat. I then added the grams of lye crystals to water. The lye and water reacted and heated up to around 120 degrees with no outside heat required. I monitored both pots and once they were both around 95 degrees I poured the lye into the fat mixture.



After combining them I stirred the mixture for about 25 minutes. Almost right away the mixture smelled like soap.



After 25 minutes the mixture thickened up. I added purple dye and lavender scent and mixed it together. It actually took a fourth of the bottle to change the color very much.



Finally, I poured it into a rusty cupcake tin which I dedicated to soap making.



Here the soap will sit for a couple days to harden up. After that I will pop them out of the tin and let them cure for a couple weeks before using them. My hope is that using lard will make the bars softer and perhaps lather better than the 100% bison mixture.

The recipe I used was:
1/2 lb. bison tallow
1/2 lb. pork lard
53.47 grams lye crystals
enough water to dissolve the lye.
dye and scent to taste.

I read online that lye crystals are no longer sold in stores because they have been used to make illegal drugs. If this is true then I will eventually run out of a critical ingredient in soap. This gives me more motivation to harvest my own lye using wood ash. I hope to experiment with that in the future.

Sunday, June 14, 2009

Bison Soap

Today I made my first ever batch of soap. My brother took a soapmaking class a number of months ago so he guided me through the process. First I looked for a recipe using bison fat but couldn't find one. I guess not many people get their hands on bison fat these days. Meanwhile my brother and I have 5-gallon buckets full. :)

I substituted beef fat when looking up how much lye to use. Hopefully I calculated it correctly. It's something you really don't want to mess around with. If your lye to fat ratio is wrong then you might end up with a chemical burn like Ed Norton in Fight Club. I had the balsamic vinegar standing by just in case.

The recipe I created was:
  • 1 cup rendered bison fat
  • 60.8 grams lye
  • 1/3 cup water
  • paprika added generously for color
  • ~ 1 teaspoon vanilla essential oil for scent
One cup of rendered bison fat from the bison we butchered.


I weighed the lye crystals on the coffee filter carefully using the electronic scale. Then I mixed them into the bowl with 1/3 cup of water on the right. The water and lye reacted chemically and heated up.



Meanwhile I melted the bison fat and started monitoring the temperature of both the fat and the lye mixture.



It took some jockeying to get both temperatures to drop to 98 degrees at the same time. I ended up chilling and reheating the fat, but eventually I zeroed in on the target temperature. Once the temperature of the fat and the lye were both around 98 degrees I poured the lye into the fat and mixed.

I stirred for about 10-15 minutes to fully mix the lye with the fat. As it cooled it started to thicken. Once a drip from the spoon lingered on the surface of the mixture I knew it was time to pour.



I quickly mixed in the paprika and vanilla oil and then poured it into a plastic mold.



I'm kind of surprised at how much the ingredients made. Now I will let these set up for 3-4 days. Then I will knock them out and let them cure for 3 weeks. Hopefully the final products will not burn me.